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      Developing an optimised method for accurate wear testing of dental materials using the ‘Rub&Roll’ device

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          Abstract

          Dental materials are challenged by wear processes in the oral environment and should be evaluated in laboratory tests prior to clinical use. Many laboratory wear-testing devices are high-cost investments and not available for cross-centre comparisons. The ‘Rub&Roll’ wear machine enables controlled application of force, chemical and mechanical loading, but the initial design was not able to test against rigid antagonist materials. The current study aimed to probe the sensitivity of a new ‘Rub&Roll’ set-up by evaluating the effect of force and test solution parameters (deionized water; water + abrasive medium; acid + abrasive medium) on the wear behaviour of direct and indirect dental resin-based composites (RBCs) compared with human molars against 3D-printed rod antagonists. Molars exhibited greater height loss than RBCs in all test groups, with the largest differences recorded with acidic solutions. Direct RBCs showed significantly greater wear than indirect RBCs in the groups containing abrasive media. The acidic + abrasive medium did not result in increased wear of RBC materials. The developed method using the ‘Rub&Roll’ wear machine in the current investigation has provided a sensitive wear test method to allow initial screening of resin-based composite materials compared with extracted human molars under the influence of different mechanical and erosive challenges.

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          From Artisanal to CAD-CAM Blocks: State of the Art of Indirect Composites.

          Indirect composites have been undergoing an impressive evolution over the last few years. Specifically, recent developments in computer-aided design-computer-aided manufacturing (CAD-CAM) blocks have been associated with new polymerization modes, innovative microstructures, and different compositions. All these recent breakthroughs have introduced important gaps among the properties of the different materials. This critical state-of-the-art review analyzes the strengths and weaknesses of the different varieties of CAD-CAM composite materials, especially as compared with direct and artisanal indirect composites. Indeed, new polymerization modes used for CAD-CAM blocks-especially high temperature (HT) and, most of all, high temperature-high pressure (HT-HP)-are shown to significantly increase the degree of conversion in comparison with light-cured composites. Industrial processes also allow for the augmentation of the filler content and for the realization of more homogeneous structures with fewer flaws. In addition, due to their increased degree of conversion and their different monomer composition, some CAD-CAM blocks are more advantageous in terms of toxicity and monomer release. Finally, materials with a polymer-infiltrated ceramic network (PICN) microstructure exhibit higher flexural strength and a more favorable elasticity modulus than materials with a dispersed filler microstructure. Consequently, some high-performance composite CAD-CAM blocks-particularly experimental PICNs-can now rival glass-ceramics, such as lithium-disilicate glass-ceramics, for use as bonded partial restorations and crowns on natural teeth and implants. Being able to be manufactured in very low thicknesses, they offer the possibility of developing innovative minimally invasive treatment strategies, such as "no prep" treatment of worn dentition. Current issues are related to the study of bonding and wear properties of the different varieties of CAD-CAM composites. There is also a crucial need to conduct clinical studies. Last, manufacturers should provide more complete information regarding their product polymerization process, microstructure, and composition, which significantly influence CAD-CAM material properties.
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            The mechanical properties of human dentin: a critical review and re-evaluation of the dental literature.

            The past 50 years of research on the mechanical properties of human dentin are reviewed. Since the body of work in this field is highly inconsistent, it was often necessary to re-analyze prior studies, when possible, and to re-assess them within the framework of composite mechanics and dentin structure. A critical re-evaluation of the literature indicates that the magnitudes of the elastic constants of dentin must be revised considerably upward. The Young's and shear moduli lie between 20-25 GPa and 7-10 GPa, respectively. Viscoelastic behavior (time-dependent stress relaxation) measurably reduces these values at strain rates of physiological relevance; the reduced modulus (infinite relaxation time) is about 12 GPa. Furthermore, it appears as if the elastic properties are anisotropic (not the same in all directions); sonic methods detect hexagonal anisotropy, although its magnitude appears to be small. Strength data are re-interpreted within the framework of the Weibull distribution function. The large coefficients of variation cited in all strength studies can then be understood in terms of a distribution of flaws within the dentin specimens. The apparent size-effect in the tensile and shear strength data has its origins in this flaw distribution, and can be quantified by the Weibull analysis. Finally, the relatively few fracture mechanics and fatigue studies are discussed. Dentin has a fatigue limit. For stresses smaller than the normal stresses of mastication, approximately 30 MPa, a flaw-free dentin specimen apparently will not fail. However, a more conservative approach based on fatigue crack growth rates indicates that if there is a pre-existing flaw of sufficient size (approximately 0.3-1.0 mm), it can grow to catastrophic proportion with cyclic loading at stresses below 30 MPa.
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              Built to last: The structure, function, and evolution of primate dental enamel

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                Author and article information

                Contributors
                eva.maier@fau.de
                Journal
                Sci Rep
                Sci Rep
                Scientific Reports
                Nature Publishing Group UK (London )
                2045-2322
                2 August 2024
                2 August 2024
                2024
                : 14
                : 17885
                Affiliations
                [1 ]GRID grid.5330.5, ISNI 0000 0001 2107 3311, Department of Operative Dentistry and Periodontology, University Hospital Erlangen, , Friedrich–Alexander Universität Erlangen–Nürnberg, ; Glueckstrasse 11, 91054 Erlangen, Germany
                [2 ]Department of Dentistry, Radboud University Medical Center, ( https://ror.org/05wg1m734) Nijmegen, The Netherlands
                [3 ]Dental and Biomaterials Science, School of Dentistry, College of Medical and Dental Sciences, University of Birmingham, ( https://ror.org/03angcq70) Birmingham, UK
                [4 ]GRID grid.5330.5, ISNI 0000 0001 2107 3311, Department of Oral and Cranio-Maxillofacial Surgery, University Hospital Erlangen, , Friedrich–Alexander Universität Erlangen–Nürnberg, ; Erlangen, Germany
                [5 ]GRID grid.5330.5, ISNI 0000 0001 2107 3311, Department of Prosthodontics, University Hospital Erlangen, , Friedrich–Alexander Universität Erlangen–Nürnberg, ; Erlangen, Germany
                Article
                68873
                10.1038/s41598-024-68873-y
                11297336
                39095406
                02c50cc4-7c41-437f-a135-62b96f074d6c
                © The Author(s) 2024

                Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/.

                History
                : 11 April 2024
                : 29 July 2024
                Funding
                Funded by: Interdisciplinary Center for Clinical Research (IZKF) at the University Hospital of the University of Erlangen-Nuremberg
                Award ID: Junior Project J103
                Award Recipient :
                Funded by: Universitätsklinikum Erlangen (8546)
                Categories
                Article
                Custom metadata
                © Springer Nature Limited 2024

                Uncategorized
                dental materials,wear,erosion,abrasion,laboratory test method,resin-based composites,dentine,enamel,experimental models of disease,preclinical research,biomedical materials,characterization and analytical techniques,scanning electron microscopy

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