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      Nanoporous Gold: Fabrication, Characterization, and Applications

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          Abstract

          Nanoporous gold (np-Au) has intriguing material properties that offer potential benefits for many applications due to its high specific surface area, well-characterized thiol-gold surface chemistry, high electrical conductivity, and reduced stiffness. The research on np-Au has taken place on various fronts, including advanced microfabrication and characterization techniques to probe unusual nanoscale properties and applications spanning from fuel cells to electrochemical sensors. Here, we provide a review of the recent advances in np-Au research, with special emphasis on microfabrication and characterization techniques. We conclude the paper with a brief outline of challenges to overcome in the study of nanoporous metals.

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          An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments

          The indentation load-displacement behavior of six materials tested with a Berkovich indenter has been carefully documented to establish an improved method for determining hardness and elastic modulus from indentation load-displacement data. The materials included fused silica, soda–lime glass, and single crystals of aluminum, tungsten, quartz, and sapphire. It is shown that the load–displacement curves during unloading in these materials are not linear, even in the initial stages, thereby suggesting that the flat punch approximation used so often in the analysis of unloading data is not entirely adequate. An analysis technique is presented that accounts for the curvature in the unloading data and provides a physically justifiable procedure for determining the depth which should be used in conjunction with the indenter shape function to establish the contact area at peak load. The hardnesses and elastic moduli of the six materials are computed using the analysis procedure and compared with values determined by independent means to assess the accuracy of the method. The results show that with good technique, moduli can be measured to within 5%.
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            Watersheds in digital spaces: an efficient algorithm based on immersion simulations

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              Survey over image thresholding techniques and quantitative performance evaluation

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                Author and article information

                Journal
                Materials (Basel)
                Materials (Basel)
                materials
                Materials
                Molecular Diversity Preservation International
                1996-1944
                03 December 2009
                December 2009
                : 2
                : 4
                : 2188-2215
                Affiliations
                [1 ]Center for Engineering in Medicine, Department of Surgery, Harvard Medical School, Massachusetts General Hospital, Shriners Hospitals for Children, Boston, MA 02114, USA
                [2 ]Department of Electrical and Computer Engineering, University of Virginia, Charlottesville, VA 22904, USA; E-Mails: reed@ 123456virginia.edu (M.L.R.); begley@ 123456virginia.edu (M.R.B.)
                [3 ]Department of Mechanical and Aerospace Engineering, University of Virginia, Charlottesville, VA 22904, USA
                [4 ]Department of Materials Science and Engineering, University of Virginia, Charlottesville, VA 22904, USA
                Author notes
                [* ]Author to whom correspondence should be addressed; E-Mail: eseker@ 123456partners.org ; Tel.: +1-434-409-9056.
                Article
                materials-02-02188
                10.3390/ma2042188
                5513576
                76f0dd80-3c02-4059-9aba-aac153dba566
                © 2009 by the authors.

                Licensee Molecular Diversity Preservation International, Basel, Switzerland. This article is an open-access article distributed under the terms and conditions of the Creative Commons Attribution license ( http://creativecommons.org/licenses/by/3.0/).

                History
                : 27 October 2009
                : 29 November 2009
                : 02 December 2009
                Categories
                Review

                nanoporous,gold,microfabrication,characterization,surface area,morphology,mems,catalyst,sensor,gold-silver alloy

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