Manganese(III) Acetate-Promoted Cross-Coupling Reaction of Benzothiazole/Thiazole Derivatives with Organophosphorus Compounds under Ball-Milling Conditions.

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Abstract

The first solvent-free manganese(III) acetate-promoted reaction of benzothiazole/thiazole derivatives with organophosphorus compounds including phosphine oxides, phosphinate ester, and phosphonate diester has been efficiently developed under ball-milling conditions, providing a highly efficient and green protocol to structurally diverse C2-phosphonylated benzothiazole/thiazole derivatives with remarkable functional group tolerance and excellent yields.

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Journal

Journal ID (iso-abbrev): J. Org. Chem.

Title: The Journal of organic chemistry

Publisher: American Chemical Society (ACS)

ISSN (Electronic): 1520-6904

ISSN (Print): 0022-3263

Publication date (Electronic): Jul 01 2016

Volume: 81

Issue: 13

Affiliations

[1 ] CAS Key Laboratory of Soft Matter Chemistry, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials), Hefei National Laboratory for Physical Sciences at Microscale, and Department of Chemistry, University of Science and Technology of China , Hefei, Anhui 230026, P. R. China.

Article

DOI: 10.1021/acs.joc.6b00786

PubMed ID: 27248000

SO-VID: 58e71375-8c1d-40c1-80bd-183543b51725

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