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      Back to the future: The advantage of studying key events in human evolution using a new high resolution radiocarbon method

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          Abstract

          Radiocarbon dating is the most widely applied dating method in archaeology, especially in human evolution studies, where it is used to determine the chronology of key events, such as the replacement of Neanderthals by modern humans in Europe. However, the method does not always provide precise and accurate enough ages to understand the important processes of human evolution. Here we review the newest method developments in radiocarbon dating (‘Radiocarbon 3.0’), which can lead us to much better chronologies and understanding of the major events in recent human evolution. As an example, we apply these new methods to discuss the dating of the important Palaeolithic site of Bacho Kiro (Bulgaria).

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          Most cited references78

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          INTCAL98 Radiocarbon Age Calibration, 24,000–0 cal BP

          The focus of this paper is the conversion of radiocarbon ages to calibrated (cal) ages for the interval 24,000–0 cal BP (Before Present, 0 cal BP = AD 1950), based upon a sample set of dendrochronologically dated tree rings, uranium-thorium dated corals, and varve-counted marine sediment. The14C age–cal age information, produced by many laboratories, is converted to Δ14C profiles and calibration curves, for the atmosphere as well as the oceans. We discuss offsets in measuredl4C ages and the errors therein, regional14C age differences, tree–coral14C age comparisons and the time dependence of marine reservoir ages, and evaluate decadalvs. single-year14C results. Changes in oceanic deepwater circulation, especially for the 16,000–11,000 cal BP interval, are reflected in the Δ14C values of INTCAL98.
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            THE INTCAL20 NORTHERN HEMISPHERE RADIOCARBON AGE CALIBRATION CURVE (0–55 CAL kBP)

            Radiocarbon ( 14 C) ages cannot provide absolutely dated chronologies for archaeological or paleoenvironmental studies directly but must be converted to calendar age equivalents using a calibration curve compensating for fluctuations in atmospheric 14 C concentration. Although calibration curves are constructed from independently dated archives, they invariably require revision as new data become available and our understanding of the Earth system improves. In this volume the international 14 C calibration curves for both the Northern and Southern Hemispheres, as well as for the ocean surface layer, have been updated to include a wealth of new data and extended to 55,000 cal BP. Based on tree rings, IntCal20 now extends as a fully atmospheric record to ca. 13,900 cal BP. For the older part of the timescale, IntCal20 comprises statistically integrated evidence from floating tree-ring chronologies, lacustrine and marine sediments, speleothems, and corals. We utilized improved evaluation of the timescales and location variable 14 C offsets from the atmosphere (reservoir age, dead carbon fraction) for each dataset. New statistical methods have refined the structure of the calibration curves while maintaining a robust treatment of uncertainties in the 14 C ages, the calendar ages and other corrections. The inclusion of modeled marine reservoir ages derived from a three-dimensional ocean circulation model has allowed us to apply more appropriate reservoir corrections to the marine 14 C data rather than the previous use of constant regional offsets from the atmosphere. Here we provide an overview of the new and revised datasets and the associated methods used for the construction of the IntCal20 curve and explore potential regional offsets for tree-ring data. We discuss the main differences with respect to the previous calibration curve, IntCal13, and some of the implications for archaeology and geosciences ranging from the recent past to the time of the extinction of the Neanderthals.
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              IntCal09 and Marine09 Radiocarbon Age Calibration Curves, 0–50,000 Years cal BP

              The IntCal04 and Marine04 radiocarbon calibration curves have been updated from 12 cal kBP (cal kBP is here defined as thousands of calibrated years before AD 1950), and extended to 50 cal kBP, utilizing newly available data sets that meet the IntCal Working Group criteria for pristine corals and other carbonates and for quantification of uncertainty in both the14C and calendar timescales as established in 2002. No change was made to the curves from 0–12 cal kBP. The curves were constructed using a Markov chain Monte Carlo (MCMC) implementation of the random walk model used for IntCal04 and Marine04. The new curves were ratified at the 20th International Radiocarbon Conference in June 2009 and are available in the Supplemental Material atwww.radiocarbon.org.
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                Author and article information

                Contributors
                Role: ConceptualizationRole: MethodologyRole: ValidationRole: VisualizationRole: Writing – original draft
                Role: InvestigationRole: ValidationRole: Writing – original draft
                Role: SupervisionRole: ValidationRole: Writing – original draft
                Role: InvestigationRole: SupervisionRole: ValidationRole: Writing – original draft
                Role: Editor
                Journal
                PLoS One
                PLoS One
                plos
                PLOS ONE
                Public Library of Science (San Francisco, CA USA )
                1932-6203
                15 February 2023
                2023
                : 18
                : 2
                : e0280598
                Affiliations
                [1 ] Department of Chemistry G. Ciamician, Alma Mater Studiorum, University of Bologna, Bologna, Italy
                [2 ] Institute for Environmental Physics, University of Heidelberg, Heidelberg, Germany
                [3 ] Department of Archaeology, Simon Fraser University, Burnaby, B.C., Canada
                [4 ] Laboratory for Ion Beam Physics, ETH Zurich, Zurich, Switzerland
                University of California Santa Cruz, UNITED STATES
                Author notes

                Competing Interests: The authors have declared that no competing interests exist.

                Author information
                https://orcid.org/0000-0002-2406-3132
                Article
                PONE-D-22-26185
                10.1371/journal.pone.0280598
                9931112
                36791053
                531f84ff-2252-4862-acf6-d785c482e79f
                © 2023 Talamo et al

                This is an open access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.

                History
                : 21 September 2022
                : 3 January 2023
                Page count
                Figures: 3, Tables: 3, Pages: 17
                Funding
                Funded by: funder-id http://dx.doi.org/10.13039/100019180, HORIZON EUROPE European Research Council;
                Award ID: 803147
                Award Recipient :
                This research was supported by the HORIZON EUROPE European Research Council Grant Number: 803147 RESOLUTION, awarded to Sahra Talamo.
                Categories
                Research Article
                Social Sciences
                Archaeology
                Archaeological Dating
                Radioactive Carbon Dating
                Research and Analysis Methods
                Chemical Characterization
                Isotope Analysis
                Radioactive Carbon Dating
                Social Sciences
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                Archaeological Dating
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