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      Keyhole threshold and morphology in laser melting revealed by ultrahigh-speed x-ray imaging

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          Abstract

          We used ultrahigh-speed synchrotron x-ray imaging to quantify the phenomenon of vapor depressions (also known as keyholes) during laser melting of metals as practiced in additive manufacturing. Although expected from welding and inferred from postmortem cross sections of fusion zones, the direct visualization of the keyhole morphology and dynamics with high-energy x-rays shows that (i) keyholes are present across the range of power and scanning velocity used in laser powder bed fusion; (ii) there is a well-defined threshold from conduction mode to keyhole based on laser power density; and (iii) the transition follows the sequence of vaporization, depression of the liquid surface, instability, and then deep keyhole formation. These and other aspects provide a physical basis for three-dimensional printing in laser powder bed machines.

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          Laser powder-bed fusion additive manufacturing: Physics of complex melt flow and formation mechanisms of pores, spatter, and denudation zones

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            In situ X-ray imaging of defect and molten pool dynamics in laser additive manufacturing

            The laser–matter interaction and solidification phenomena associated with laser additive manufacturing (LAM) remain unclear, slowing its process development and optimisation. Here, through in situ and operando high-speed synchrotron X-ray imaging, we reveal the underlying physical phenomena during the deposition of the first and second layer melt tracks. We show that the laser-induced gas/vapour jet promotes the formation of melt tracks and denuded zones via spattering (at a velocity of 1 m s−1). We also uncover mechanisms of pore migration by Marangoni-driven flow (recirculating at a velocity of 0.4 m s−1), pore dissolution and dispersion by laser re-melting. We develop a mechanism map for predicting the evolution of melt features, changes in melt track morphology from a continuous hemi-cylindrical track to disconnected beads with decreasing linear energy density and improved molten pool wetting with increasing laser power. Our results clarify aspects of the physics behind LAM, which are critical for its development.
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              Real-time monitoring of laser powder bed fusion process using high-speed X-ray imaging and diffraction

              We employ the high-speed synchrotron hard X-ray imaging and diffraction techniques to monitor the laser powder bed fusion (LPBF) process of Ti-6Al-4V in situ and in real time. We demonstrate that many scientifically and technologically significant phenomena in LPBF, including melt pool dynamics, powder ejection, rapid solidification, and phase transformation, can be probed with unprecedented spatial and temporal resolutions. In particular, the keyhole pore formation is experimentally revealed with high spatial and temporal resolutions. The solidification rate is quantitatively measured, and the slowly decrease in solidification rate during the relatively steady state could be a manifestation of the recalescence phenomenon. The high-speed diffraction enables a reasonable estimation of the cooling rate and phase transformation rate, and the diffusionless transformation from β to α ’ phase is evident. The data present here will facilitate the understanding of dynamics and kinetics in metal LPBF process, and the experiment platform established will undoubtedly become a new paradigm for future research and development of metal additive manufacturing.
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                Author and article information

                Journal
                Science
                Science
                American Association for the Advancement of Science (AAAS)
                0036-8075
                1095-9203
                February 21 2019
                February 22 2019
                February 21 2019
                February 22 2019
                : 363
                : 6429
                : 849-852
                Article
                10.1126/science.aav4687
                30792298
                49feccd4-25aa-46cf-9099-ce2484363855
                © 2019

                http://www.sciencemag.org/about/science-licenses-journal-article-reuse

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