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      Anneal-free ultra-low loss silicon nitride integrated photonics

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          Abstract

          Heterogeneous and monolithic integration of the versatile low-loss silicon nitride platform with low-temperature materials such as silicon electronics and photonics, III–V compound semiconductors, lithium niobate, organics, and glasses has been inhibited by the need for high-temperature annealing as well as the need for different process flows for thin and thick waveguides. New techniques are needed to maintain the state-of-the-art losses, nonlinear properties, and CMOS-compatible processes while enabling this next generation of 3D silicon nitride integration. We report a significant advance in silicon nitride integrated photonics, demonstrating the lowest losses to date for an anneal-free process at a maximum temperature 250 °C, with the same deuterated silane based fabrication flow, for nitride and oxide, for an order of magnitude range in nitride thickness without requiring stress mitigation or polishing. We report record low anneal-free losses for both nitride core and oxide cladding, enabling 1.77 dB m -1 loss and 14.9 million Q for 80 nm nitride core waveguides, more than half an order magnitude lower loss than previously reported sub 300 °C process. For 800 nm-thick nitride, we achieve as good as 8.66 dB m −1 loss and 4.03 million Q, the highest reported Q for a low temperature processed resonator with equivalent device area, with a median of loss and Q of 13.9 dB m −1 and 2.59 million each respectively. We demonstrate laser stabilization with over 4 orders of magnitude frequency noise reduction using a thin nitride reference cavity, and using a thick nitride micro-resonator we demonstrate OPO, over two octave supercontinuum generation, and four-wave mixing and parametric gain with the lowest reported optical parametric oscillation threshold per unit resonator length. These results represent a significant step towards a uniform ultra-low loss silicon nitride homogeneous and heterogeneous platform for both thin and thick waveguides capable of linear and nonlinear photonic circuits and integration with low-temperature materials and processes.

          Abstract

          We demonstrate for the first time, a uniform low temperature (<250 °C) process for fabricating both high-confinement thick and low-confinement thin ultra-low loss Silicon nitride waveguides.

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          Dissipative Kerr solitons in optical microresonators

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              Photonic-chip-based frequency combs

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                Author and article information

                Contributors
                danb@ucsb.edu
                Journal
                Light Sci Appl
                Light Sci Appl
                Light, Science & Applications
                Nature Publishing Group UK (London )
                2095-5545
                2047-7538
                8 July 2024
                8 July 2024
                2024
                : 13
                : 156
                Affiliations
                [1 ]Department of Electrical and Computer Engineering, University of California Santa Barbara, ( https://ror.org/02t274463) Santa Barbara, CA 93106 USA
                [2 ]Octave Photonics, Louisville, CO 80027 USA
                Author information
                http://orcid.org/0009-0003-2590-0582
                http://orcid.org/0000-0002-5373-4396
                http://orcid.org/0000-0002-1360-9646
                http://orcid.org/0000-0002-5796-5220
                http://orcid.org/0000-0002-7375-3690
                http://orcid.org/0000-0002-1735-7220
                Article
                1503
                10.1038/s41377-024-01503-4
                11231177
                38977674
                2990ad02-4776-4222-89f6-9ef3fd5635ab
                © The Author(s) 2024

                Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/.

                History
                : 15 February 2024
                : 1 June 2024
                : 10 June 2024
                Funding
                Funded by: FundRef https://doi.org/10.13039/100000185, United States Department of Defense | Defense Advanced Research Projects Agency (DARPA);
                Award ID: HR0011-22-2-0008
                Award Recipient :
                Funded by: FundRef https://doi.org/10.13039/100006754, United States Department of Defense | United States Army | U.S. Army Research, Development and Engineering Command | Army Research Laboratory (U.S. Army Research Laboratory);
                Award ID: W911NF-22-2-0056
                Award Recipient :
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                © Changchun Institute of Optics, Fine Mechanics and Physics (CIOMP), CAS 2024

                optical materials and structures,supercontinuum generation,optical metrology

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